Research use only.  Educational reference. Not medical advice. Not for human consumption.
⚖️ GLP-1 Agonist

Semaglutide (5 mg Vial) Dosage Protocol

Semaglutide is a long-acting GLP-1 receptor agonist studied in landmark Phase 3 trials (STEP, SUSTAIN). Standard maintenance for weight protocols is 2.4 mg weekly. This page covers the 5 mg vial.

⚡ Quickstart Highlights

Vial size
5 mg
Reconstitution
3 mL BAC water → 1.67 mg/mL
1 U-100 unit =
16.7 mcg
Frequency
Once weekly

Dosing & Reconstitution Guide

Route: Subcutaneous  |  Frequency: Once weekly  |  Half-life: ~7 days

Standard Approach (3 mL = 1.67 mg/mL)

Reconstituting with 3 mL bacteriostatic water produces a concentration of 1.67 mg/mL. Volume per dose changes with concentration; mg dose itself does not change between vial sizes.

Phase / ProtocolDoseU-100 UnitsVolumeDoses per vial
Weeks 1–4 (titration)250 mcg15 units0.15 mL20 doses
Weeks 5–8500 mcg30 units0.30 mL10 doses
Weeks 9–121 mg60 units0.60 mL5 doses
Weeks 13–161.7 mg102 units1.02 mL2 doses
Weeks 17+ (maintenance)2.4 mg144 units1.44 mL2 doses

Reconstitution Steps

  1. Wipe the vial stopper and BAC water vial with alcohol; let dry.
  2. Draw 3 mL of bacteriostatic water into a sterile syringe.
  3. Inject slowly down the inside glass wall of the peptide vial. Do not aim at the powder.
  4. Gently swirl until fully dissolved. Do not shake.
  5. Label with reconstitution date. Refrigerate at 2–8°C; use within 28 days.

Supplies Needed

Estimates for an 8-week and 12-week cycle at 2.4 mg per dose, once weekly (1 dose/week).

Item8-Week Cycle12-Week Cycle
Semaglutide (5 mg) vials4 vials6 vials
Insulin syringes (U-100)812
Bacteriostatic water (10 mL)2 × 10 mL2 × 10 mL
Alcohol swabs1 × 100-pack2 × 100-pack

Protocol Overview

The STEP-1 protocol — the original landmark obesity trial — uses a 4-step titration over 16 weeks before reaching the 2.4 mg maintenance dose. Semaglutide's once-weekly dosing and 7-day half-life make it forgiving on timing but slow to clear if side effects become a problem.

Most research protocols run 6–18 months. In STEP-1 the weight-loss curve was still trending downward at week 68 (final measurement), suggesting longer protocols may produce additional benefit.

Cycle length: Continuous use for 6–18 months in most protocols. Some users transition to a "maintenance" 1.0–1.7 mg weekly dose after reaching target, rather than the full 2.4 mg, to preserve results with reduced side-effect load.

What to expect by week: Weeks 1–4 — mild appetite suppression begins. Weeks 5–16 — titration phase, weight-loss curve gradually steepens. Weeks 17–32 — primary weight-loss phase. Weeks 32+ — gradual continued loss, plateau approach.

Dosing Protocol

Standard STEP-1 obesity protocol — 4-week titration intervals:

SUSTAIN T2DM protocol: Same titration steps but maintenance often at 1.0 mg weekly, which produced the cardiovascular benefit in SUSTAIN-6.

Slower titration variant: Some research protocols hold each step for 6–8 weeks instead of 4 if GI tolerability is poor. This extends the time to maintenance but reduces dropout from side effects.

Day-of-week timing: Same day each week. Half-life ~7 days — the longest of the GLP-1 class. Doses can shift ±2 days without affecting steady state.

Missed dose: ≤5 days late, take when remembered. >5 days, skip and resume next scheduled day.

Maintenance reduction: Once at target weight, many users drop to 1.7 mg or 1.0 mg weekly indefinitely to maintain results with fewer side effects.

Storage Instructions

StateTemperatureDuration
Lyophilized−20°C (−4°F)Up to 24 months, dry & dark
Reconstituted2–8°C (35–46°F)Up to 28 days, protect from light

Important Notes

⚠ Research Use Only: Semaglutide is approved internationally as a prescription medication. Research-grade compounded material is investigational.

How This Works

Semaglutide is a 31-amino-acid synthetic analog of native GLP-1. Two modifications give it a half-life of ~7 days vs minutes for native GLP-1: substitution of alanine at position 8 (preventing DPP-4 degradation) and a fatty-acid linker that binds albumin.

It activates GLP-1 receptors in pancreatic beta cells (enhancing insulin secretion), the hypothalamus (suppressing appetite), and the gut (slowing gastric emptying). Insulin response is glucose-dependent, so hypoglycemia risk is low as monotherapy.

Potential Benefits & Side Effects

Potential Benefits

Side Effect Profile

Lifestyle Factors

Injection Technique

References

1
Wilding JPH et al. 'Once-Weekly Semaglutide in Adults with Overweight or Obesity' (STEP 1) — NEJM, 2021 View source ↗
2
Marso SP et al. 'Semaglutide and Cardiovascular Outcomes' (SUSTAIN-6) — NEJM, 2016 View source ↗